The Zeiss AxioImager Z1.m and Keyence VHX-1000 optical microscopes are available for the service. Particular requests shall be discussed with operators in advance
Rozcestník experimentálního vybavení pro fyziku a materiálové vědy
Research services
4.2.1. Scanning electron microscopy services
Services using Tescan FERA 3 electron microscope
Both secondary electrons and back-scattered electrons detectors can be used with nominal resolution 2 nm at least. Non-conductive or poorly conductive samples can be observed by beam deceleration mode or low-vacuum microscopy working at nitrogen atmosphere with the pressure up to 500 Pa and resolution i3,5 nm. Particular requests shall be discussed with operators in advance
Contact: J. Kopeček / 2899 / kopecek@fzu.cz
4.2.1. 3D microstructure and microtexture characterisation
Microstructure and microtexture characterisation of bulk materials by the application of FIB sectioning method with electron back-scattered diffraction method using EDAC Digiview V analyzer on Tescan FERA 3 SEM can be used to map the crystal lattice orientation and evaluate consequent quantities (texture, grain size, grain boundary characteristics etc.). The metallographically polished surface or other fresh crystalline surface (deposited layers) is requested. Limited amount of samples can be prepared in the metalography laboratory.
Contact: J. Kopeček / 2899 / kopecek@fzu.cz
4.2.1. Analysis of chemical composition
Analysis of chemical composition using the energy-dispersive spectroscopy (EDS) analyzer on Tescan FERA 3 SEM can be made in semi-quantitative mode. Samples with polished surfaces are required. Limited sample preparation can be made in the laboratory. particular requests shall be discussed with operators in advance.
Contact: J. Kopeček / 2899 / kopecek@fzu.cz
4.2.1. Design and testing of active NiTi elements for smart structures
We offer designing, testing, heat treating and shape setting of elements made from NiTi based shape memory alloys (wires, ribbons, springs, sheets, bars) to be used as components of smart structures (superelastic members, thermally driven actuators, vibration dampers) for automotive, medical device or civil engineering aplications.
Contact: Luděk Heller / 266052428 / heller@fzu.cz
4.2.1. Electrochemical characterisation of surfaces and corrosion testing
Characterisation of material surfaces and corrosion testing by electrochemical methods (Open Circuit Potential, Potenciostatic and Potentiodynamic polarization, Electrochemical Impedance Spectroscopy, In situ measurements under applied stress or during mechanical loads)
Contact: J. Racek / 2361 / racek@fzu.cz